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Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (07.08.2019)
Winter semester 2019/2020 The subject will be taught in English in similar way as last year. Individual lectures will be specified in the middle of October 2019 according to number of enrolled students. ************************************************************************************************************************************************************************************* Winter semester 2018/2019 ******************************* This course is specialized on the presentation of different topics of modern analytical spectrometry. It covers progresses in both molecular and atomic spectrometry. Individual topics are characterized in the syllabus. All lectures are given in English. Attendance at these lectures assumes a basic knowledge of analytical spectrometric methods (subjects MC230P04N or its equivalents and MC230P19). This course is primarily recommended for the pre-gradual, doctoral students and Erasmus students. Winter semester, 2018 Tuesday, from 9:50 a.m. in the library of the Department of Analytical Chemistry (no. 117) Speakers: RNDr. Václav Červený, Ph.D. cerveny2@natur.cuni.cz RNDr. Jakub Hraníček, Ph.D. hranicek.jakub@natur.cuni.cz Department of Analytical Chemistry, Faculty of Science, Charles University RNDr. Jan Srbek, Ph.D. jan.srbek@zentiva.cz Department of Mass Spectrometry, Zentiva k.s., a Sanofi Company RNDr. Jan Kratzer, Ph.D. jkratzer@biomed.cas.cz RNDr., Mgr. Tomáš Matoušek, Ph.D. matousek@biomed.cas.cz Institute of Analytical Chemistry of the AS CR, v.v.i., Brno Department of Trace Element Analysis, detached laboratory Prague, Czech Republic Program: 07.11. Information meeting, organization 14.11. Miniaturization of Flow Analysis Methods with Spectrometric Detection (Flow Injection Analysis, Sequential Injection Analysis, Bead Injection) 21.11. Sample preparations / analysis without sampling, Excitation Sources / Ionization Sources in Analytical Spectrometry 28.11. Volatile compounds generation (chemical, electrochemical and UV-photochemical way), High resolution continuous source atomic absorption spectrometry -towards to simultaneous AAS 05.12. Half-day excursion to the Institute of Analytical Chemistry of Academy of Science, Prague • Advanced approaches to analyte sampling - possibilities and limitations (solids and slurries, electrothermal vaporization, slurry nebulization, generation of volatile compounds) • Advanced approaches to preconcentration of analytes (especially metals) prior spectrometric detection (cloud point extraction, dispersed liquid-liquid microextraction, magnetic and nanometer-sized materials as sorbents, electrodeposition, solid phase extraction, in-situ trapping of volatile compounds) • Miniature and low power atmospheric plasmas as sources of ions, atoms and excited atoms • Element speciation analysis (principles, methods, applications according to elements) • Tour in the IAC laboratories. 12.12. Ion sources - interface technology (electrospray, APCI/APPI), LC-MS spectra demonstration/differences, Mass spectrometer HW introduction (ionization source, ion optics, analyzers, detectors), Mass analyzers/tandem MS (Q, QQQ, Ion Trap, (Q)-TOF, Orbitrap) – applications, differences, pros and cons, Transfer of the Method from HPLC-UV to LC-MS, New ionization techniques DART and MALDI Srbek 19.12. Surface Analysis (Static and Dynamic Secondary Ions Mass Spectrometry, Secondary Neutral Mass Spectrometry, Rutherford Backscattering Spectroscopy, Low-Energy Ion Spectrometry, TR and ED X-ray Spectroscopy, Laser Induce Breakdown Spectroscopy) 09.01. Written examination |
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Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (07.08.2019)
Handbook of High-resolution Spectroscopy. Wiley 2011 Elektronické materiály jsou dostupné přímo v aplikaci SIS. Electronic materials are avaible here in SIS application. |
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Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (30.10.2017)
This subject will be finished by a written exam. The exam will covered all topics lectured during the session. |
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Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (07.08.2019)
1. Highly sensitive modern detectors for UV/VIS spectrum
The lecture is taught in English for Erasmus students. |