Methods of Organic Structures Elucidation - GAF405

• Anglický název: Methods of Organic Structures Elucidation
• Zajišťuje: Katedra organické a bioorganické chemie (16-16120)
• Fakulta: Farmaceutická fakulta v Hradci Králové
• Platnost: od 2024
• Semestr: letní
• Body: 0
• E-Kredity: 2
• Způsob provedení zkoušky: letní s.:
• Rozsah, examinace: letní s.:0/28, Z+Zk [HS]
• Počet míst: neurčen / neomezen (10)
• Minimální obsazenost: neomezen
• 4EU+: ne
• Virtuální mobilita / počet míst pro virtuální mobilitu: ne
• Stav předmětu: vyučován
• Jazyk výuky: angličtina
• Způsob výuky: prezenční
• Poznámka: odhlásit z termínu zkoušky při nesplněné rekvizitě; předmět je možno zapsat mimo plán; povolen pro zápis po webu
• Garant: doc. Dr. Russell Richard Anthony Kitson
• Prerekvizity : GAF301
• Záměnnost : GAF385

Anotace

čeština

n/a - see GF405

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)

angličtina

The subject is both theoretical (deepening of knowledge of spectral methods, especially NMR, then MS, IR and other methods used in many areas of chemical research), and practical (evaluation of NMR, IR, MS, ... data with an emphasis on identification of unknown compounds, correct interpretation and recording of characterization according to scientific standards). Students completing this subject will be prepared for the following scientific activity (diploma thesis, postgraduate studies, ...) and future career (pharmaceutical industry).

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)

Podmínky zakončení předmětu

čeština

n/a - see GF405

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)

angličtina

60% average across assessed work components and 100% attendance for credit. Exam grades 1-4

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)

Sylabus

čeština

n/a - see GF405

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)

angličtina

Theoretical part:

• properties of matter, separation, izolation of compounds
• NMR, IR, MS, HR-MS, CHN analysis, polarimetry
• X-ray crystallography
• EMS, circular dichroism
• identification of chiral compounds

Practical part:

• interpretation of 1D NMR spectra
• interpretation of IR and MS spectra
• interpretation of other data (chiral compounds, dr, de, er, ee, etc.)
• identification of unknown compounds
• characterization of coumpounds

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)

Výsledky učení

   

LEARNING OUTCOMES
(By the end of the module the student should….)	Which teaching and learning methods enable students to achieve this learning outcome?	Which assessment method(s) will measure the achievement of this learning outcome?
Have a good understanding of the output of various advanced spectroscopic and spectrometric analytical techniques used for organic structure elucidation.    Be able to decipher simple-complex NMR multiplets.     Be able to decipher the identity of an unknown compound from the given spectral and reaction data/information.   Be able to report data in a publishable format, including full structural assignment.	Series of seminar/lecture sessions to train students in the interpretation of spectral outputs.     Series of seminar sessions to train students in the interpretation of spectral outputs.     Series of seminar sessions to train students in the interpretation of spectral outputs.   Series of seminar sessions to train students in the interpretation of spectral outputs.	Series of homework assignments. Final exam test.     Series of homework assignments. Final exam test.      Series of homework assignments. Final exam test.     Series of homework assignments. Final exam test.

Poslední úprava: Kitson Russell Richard Anthony, doc. Dr. (14.03.2025)