Advances in Analytical Spectrometric Methods - MC230P65

• Anglický název: Advances in Analytical Spectrometric Methods
• Zajišťuje: Katedra analytické chemie (31-230)
• Fakulta: Přírodovědecká fakulta
• Platnost: od 2015 do 2019
• Semestr: zimní
• E-Kredity: 3
• Způsob provedení zkoušky: zimní s.:písemná
• Rozsah, examinace: zimní s.:2/0, Zk [HT]
• Počet míst: neomezen
• Minimální obsazenost: neomezen
• 4EU+: ne
• Virtuální mobilita / počet míst pro virtuální mobilitu: ne
• Stav předmětu: vyučován
• Jazyk výuky: angličtina
• Úroveň: specializační
• Poznámka: povolen pro zápis po webu
• Garant: RNDr. Jakub Hraníček, Ph.D.
• Vyučující: RNDr. Václav Červený, Ph.D.; RNDr. Jakub Hraníček, Ph.D.; RNDr. Jan Kratzer, Ph.D.; RNDr. Mgr. Tomáš Matoušek, Ph.D.

Anotace

Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (14.10.2016)

This course is specialized on the presentation of different topics of modern analytical spectrometry. It covers progresses in both molecular and atomic spectrometry. Individual topics are characterized in the syllabus. All lectures are given in English. Attendance at these lectures assumes a basic knowledge of analytical spectrometric methods (subjects MC230P45 or its equivalents and MC230P19). This course is primarily recommended for the pre-gradual and doctoral students.

Winter semester, 2015
Tuesday, from 9:00 a.m. in the library of the Department of Analytical Chemistry (no. 117)

Speakers:
RNDr. Václav Červený, Ph.D. [e-mail]
RNDr. Jakub Hraníček, Ph.D. [e-mail]
RNDr. Jan Kratzer, Ph.D. [e-mail]
RNDr., Mgr. Tomáš Matoušek, Ph.D. [e-mail]
RNDr. Petr Kozlík, Ph.D. [e-mail]

Program:

3.11. Sample preparations / analysis without sampling, Excitation Sources / Ionization Sources in Analytical Spectrometry Červený

10.11. Volatile compounds generation (chemical, electrochemical and UV-photochemical way), High-resolution continuous source atomic absorption spectrometry -towards to simultaneous AAS Červený

24.11. Miniaturization of Flow Analysis Methods with Spectrometric Detection (Flow injection Analysis, Sequential Injection Analysis, Bead Injection) Hraníček

1.12. Spectrometric detection in separation sciences: Ion sources - ESI, APCI, APPI; Mass analyzers; Development of LC-MS method; Applications; New ionization techniques; Trends in MS Kozlík

8.12. Half-day excursion to the Institute of Analytical Chemistry of Academy of Science, Prague
Advanced approaches to analyte sampling - possibilities and limitations (solids and slurries, generation of volatile compounds), preconcentration of metals prior spectrometric detection (cloud point extraction, electrodeposition, solid phase extraction, in-situ trapping of volatile compounds), atomization of volatile compounds - advanced atomizers (miniature plasma sources, dielectric barrier discharges). Element speciation analysis (principles, methods, applications according to elements) + tour in the IAC laboratories. Kratzer, Matoušek

15.12. Surface Analysis (Static and Dynamic Secondary Ions Mass Spectrometry, Secondary Neutral Mass Spectrometry, Rutherford Backscattering Spectroscopy, Low-Energy Ion Spectrometry, TR and ED X-ray Spectroscopy, Laser Ablation, Laser Induce Breakdown Spectroscopy) Hraníček

5.1. Remote Research of the Universe: Challenge for Analytical Chemistry Hraníček

12.1. Written examination






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2016/2017
The subject will be taught in English in similar way as last year (see bellow). Individual lectures will be specified at the beginning of October2015 according to number of enrolled students.

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Literatura

Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (14.10.2016)

Handbook of High-resolution Spectroscopy. Wiley 2011
Laser Chemistry. Spectroscopy, Dynamics and Applications. Wiley 2007
Surface Enhanced Raman Spectroscopy. Analytical, Bioanalytical and Life Science Application. Wiley 2010
Modern Spectroscopy. 4th Ed. Wiley 2004
Vzhledem k aktuálnosti probíraných témat jsou doporučovány též aktuální články z odborných časopisů.

Elektronické materiály jsou dostupné přímo v aplikaci SIS.

Electronic materials are avaible here in SIS application.

Požadavky ke zkoušce

Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (14.10.2016)

This subject will be finished by a written exam. The exam will covered all topics lectured during the session.

Sylabus

Poslední úprava: RNDr. Jakub Hraníček, Ph.D. (24.10.2017)

1. Highly sensitive modern detectors for UV/VIS spectrum
2. Laser analytical chemistry
3. High-resolution continuous source atomic absorption spectrometry - towards to simultaneous AAS
4. Microwave spectroscopy and remote research of the Universe
5. New types of mass analyzers
6. Advances in optical sensors constructions
7. Using high-frequency electromagnetic fields in medical imaging techniques
8. Spectroscopy of surface enhanced Raman scattering
9. Surface analysis by ion beams
10.New possibilities in X-ray spectrometry
11.Radioanalytical spectral techniques
12.Miniaturization of flow analysis methods with spectrometric detection

 

The lecture is taught in English for Erasmus students.