SubjectsSubjects(version: 953)
Course, academic year 2023/2024
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Instrumental Methods in Inorganic Chemistry - MC240C26
Title: Praktikum z fyzikálních metod studia anorganických látek
Czech title: Praktikum z fyzikálních metod studia anorganických látek
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2022
Semester: summer
E-Credits: 9
Examination process: summer s.:
Hours per week, examination: summer s.:0/6, MC [HT]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: taught
Language: Czech
Is provided by: MC240C15
Explanation: v plánech je nahrazeno anglickou verzí MC240C15
Guarantor: doc. RNDr. Róbert Gyepes, Dr., Ph.D.
Teacher(s): RNDr. Ivana Císařová, CSc.
doc. RNDr. Róbert Gyepes, Dr., Ph.D.
doc. RNDr. David Havlíček, CSc.
prof. RNDr. Petr Hermann, Dr.
prof. RNDr. Jana Kalbáčová Vejpravová, Ph.D.
doc. RNDr. Vojtěch Kubíček, Ph.D.
RNDr. Alan Liška, Ph.D.
prof. RNDr. Jiří Mosinger, Ph.D.
prof. RNDr. Ivan Němec, Ph.D.
RNDr. Jiří Schulz, Ph.D.
Class: Sestava HPLC-MS
Co-requisite : MC240P15
Incompatibility : MC240C15
Is incompatible with: MC240C15, MC240C14
Annotation -
The laboratory course is aimed at providing practical experiences and a brief survey of principles and applications of physical methods used in inorganic chemistry.

The course is designed for Master and PhD students.
Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (13.05.2021)
Literature -

Luerature is recommended by supervisors of selected exercises.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (26.10.2019)
Requirements to the exam -

Protocols of individual excercises are to be submitted to their leaders for inspection always within one week upon completing any excersize.

After the completion of all excersises prescribed, their acepted and signed protocols have to be delivered to the course supervisor within three weeks.

The classification of individual protocols will reflect not only the protocol quality, but also their timely submission.

 

In the case of timely protocol submission to the course supervisor, the final classification is calculated as the average of classifications achieved within all individual excerises.

In case of later submission without proving a serious reason, the final classification is worsened by one degree with respect to the classification for a timely submission.

Should the delay in submitting the protocols exceed two months for no serious reason, the final classification obtained from averaging the individual classifications will be worsened by two degrees.

Last update: Gyepes Róbert, doc. RNDr., Dr., Ph.D. (28.10.2019)
Syllabus -

This practical course consists of nine compulsory exercises and four further excersizes to be selected from a group.

Compulsory exercises:

1.    Quantitative analysis using X-ray power diffration
2.    Structure analysis using single-crystal X-ray diffraction
3.    Vibrational spectroscopy I. (IR + Raman)
4.    NMR spectroscopy
5.    Potentiometry
6.    Electronic spectroscopy

Selectable exercises:

Each student chooses four additional exercises from the below list. Venue dates are set individually after discussing with the exercise heads within one week following the introductory instruction.

7.    High-temperature powder X-ray diffraction
8.    Vibrational spectroscopy II. (IR + Raman microspectroscopy)
9.    Magnetochemistry
10.    Study of phase transitions by IR spectroscopy
11.    Study of phase transitions by Raman spectroscopy
12.    Thermal capacity of solid-state compounds – thermal dependence
13.    Magnetic phase transitions
14.    EPR spectroscopy
15.    Fluorimetry
16.    Application of quantum-chemical methods for studying physical and chemical properties
17.    Voltammetric methods
18.    Hyperthermy of magnetic nanoparticles
19.    Basic ferromagnet characteristics
20.    High performance liquid chromatography with mass detection

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (01.06.2021)
 
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