SubjectsSubjects(version: 901)
Course, academic year 2022/2023
  
Instrumental Methods in Inorganic Chemistry - MC240C15
Title: Instrumental Methods in Inorganic Chemistry
Czech title: Praktikum z fyzikálních metod studia anorganických látek
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2022
Semester: summer
E-Credits: 9
Examination process: summer s.:
Hours per week, examination: summer s.:0/6 MC [hours/week]
Capacity: unlimited
Min. number of students: unlimited
Virtual mobility / capacity: no
State of the course: taught
Language: English
Note: enabled for web enrollment
Guarantor: doc. RNDr. Róbert Gyepes, Dr., Ph.D.
Class: Sestava HPLC-MS
Původní předmět
Co-requisite : MC240P15
Incompatibility : MC240C26
Is incompatible with: MC240C26
Opinion survey results   Examination dates   Schedule   
Annotation -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (06.05.2021)
The laboratory course is aimed at providing practical experiences and a brief survey of principles and
applications of physical methods used in inorganic chemistry.

The course is designed for Master and PhD students.
Literature -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (06.05.2021)

Luerature is recommended by supervisors of selected exercises.

Requirements to the exam -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (06.05.2021)

Protocols of individual excercises are to be submitted to their leaders for inspection always within one week upon completing any excersize.

After the completion of all excersises prescribed, their acepted and signed protocols have to be delivered to the course supervisor within three weeks.

The classification of individual protocols will reflect not only the protocol quality, but also their timely submission.

 

In the case of timely protocol submission to the course supervisor, the final classification is calculated as the average of classifications achieved within all individual excerises.

In case of later submission without proving a serious reason, the final classification is worsened by one degree with respect to the classification for a timely submission.

Should the delay in submitting the protocols exceed two months for no serious reason, the final classification obtained from averaging the individual classifications will be worsened by two degrees.

Syllabus -
Last update: doc. RNDr. Vojtěch Kubíček, Ph.D. (13.05.2021)

This practical course consists of nine compulsory exercises and four further excersizes to be selected from a group.

Compulsory exercises:

1.    Quantitative analysis using X-ray power diffration
2.    Structure analysis using single-crystal X-ray diffraction
3.    Vibrational spectroscopy I. (IR + Raman)
4.    NMR spectroscopy
5.    Potentiometry
6.    Electronic spectroscopy

Selectable exercises:

Each student chooses four additional exercises from the below list. Venue dates are set individually after discussing with the exercise heads within one week following the introductory instruction.

7.    High-temperature powder X-ray diffraction
8.    Vibrational spectroscopy II. (IR + Raman microspectroscopy)
9.    Magnetochemistry
10.    Study of phase transitions by IR spectroscopy
11.    Study of phase transitions by Raman spectroscopy
12.    Thermal capacity of solid-state compounds – thermal dependence
13.    Magnetic phase transitions
14.    EPR spectroscopy
15.    Fluorimetry
16.    Application of quantum-chemical methods for studying physical and chemical properties
17.    Voltammetric methods
18.    Hyperthermy of magnetic nanoparticles
19.    Basic ferromagnet characteristics
20.    High performance liquid chromatography with mass detection

 
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