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Course, academic year 2016/2017
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Applied Structure Analysis - NFPL040
Title: Aplikovaná strukturní analýza
Guaranteed by: Department of Condensed Matter Physics (32-KFKL)
Faculty: Faculty of Mathematics and Physics
Actual: from 2015
Semester: summer
E-Credits: 3
Hours per week, examination: summer s.:1/1, C+Ex [HT]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: taught
Language: Czech
Teaching methods: full-time
Teaching methods: full-time
Additional information: http://krystal.karlov.mff.cuni.cz/FPL040
Guarantor: doc. RNDr. Stanislav Daniš, Ph.D.
Classification: Physics > Solid State Physics
Annotation -
Last update: T_KFES (23.05.2001)
This lecture is intended to diploma and PhD students specialised in the X-ray diffraction. The lecture is an extension of lectures FPL012 (Structure of matter and diffraction of radiation) and FPL030 (Diffraction methods). It covers the following topics: (a) treatment of instrumental phenomena in X-ray diffraction, (b) study of temperature atomic vibrations, (c) study of chemical inhomogeneities and diffusion processes, (d) diffraction on thin films, (e) diffraction on low -dimensionally periodic structures (multilayers, quantum dots) and (e) some computational methods in structure analysis. The complete course on advanced methods in X-ray diffraction consists of two lectures: FPL029 (X-ray diffraction study of the real structure of matter) and FPL040.
Syllabus -
Last update: T_KFES (26.05.2003)

1. Accuracy in diffraction experiment - instrumental aberrations, microstructural parameters, geometrical factors, sample transparency, absorption of x-rays, surface roughness, primary and secondary extinction, preferred orientation of crystallites

2. Dynamical effects in crystals.Thermal vibrations, diffusion, chemical inhomogeneity

3. Short and long range ordering - diffractional study of local arrangement at phase transition, x-ray diffraction on structures with large periodicity (multilayers, superconductors) high and low angle diffraction, reflectivity (optical theory, DBWA)

4. Experimental methods of determining the short range orderining - EXAFS, diffuse scattering

5. Computional methods in applied structural analysis - simulating of diffraction pattern (Lazy Pulverix), refinement of real crystal structure (the Rietveld method), deconvolution. Determinination of thin film, multilayer and superconductor structure parameters (SUPREX)

 
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