Subjects

Your browser does not support JavaScript, or its support is disabled. Some features may not be available.

Advances in Analytical Spectrometric Methods - MC230P65

Title:	Advances in Analytical Spectrometric Methods
Guaranteed by:	Department of Analytical Chemistry (31-230)
Faculty:	Faculty of Science
Actual:	from 2023
Semester:	summer
E-Credits:	3
Examination process:	summer s.:written
Hours per week, examination:	summer s.:2/0, Ex [HT]
Capacity:	unlimited
Min. number of students:	unlimited
4EU+:	no
Virtual mobility / capacity:	no
State of the course:	taught
Language:	English
Level:	specialized
Note:	enabled for web enrollment

Guarantor:	RNDr. Jan Kratzer, Ph.D.
Teacher(s):	RNDr. Václav Červený, Ph.D. RNDr. Jakub Hraníček, Ph.D. RNDr. Jan Kratzer, Ph.D. RNDr. Mgr. Tomáš Matoušek, Ph.D.

Opinion survey results Examination dates SS schedule

Annotation -

Last update: RNDr. Jan Kratzer, Ph.D. (14.02.2024)

This course is taught in English for Erasmus and PhD students. New trends and techniques in the fields of atomic and molecular spectroscopy and mass spectrometry are discussed including their applications. Also advanced approaches to sample preparation and preconcentration are presented. Lectures are accompanied by excursions to selected laboratories whenever possible. Practical demonstrations of analytical measurements using state-of-the-art spectrometric instrumentation will be shown. The series of lectures is given by experienced researchers from Czech universities and Czech Academy of Sciences. Basic knowledge of fundamental spectroscopic techniques is expected. Active participation of the students is expected with maximum absence of 20%.

The course starts on Wednesday 21 February 2024. The schedule of lectures and excursions will be specified after agreement regarding the students' time availability during the first week of semester.

Programme for first three weeks of summer semester 2024 (the dates and speakers are confirmed):

Date Lecturer Topic Institution
21.2. RNDr. Jan Kratzer, Ph.D. Introduction to atomic, molecular and mass spectrometry IAC CAS
28.2. RNDr. Tomáš Matoušek, Ph.D. Elemental speciation analysis IAC CAS
6.3. RNDr. Václav Červený, Ph.D. Spectrometric analysis without sample preparation FS CU

Following invited speakers will also deliver their lectures accompanied always by demonstration of analytical spectrometric instrumentation and real measurements. The dates of their talks/excursions will be specified later, based on the agreement with the students, but well in advance:

Assoc. Prof. Ing. Antonín Kaňa, Ph.D. Single particle ICP-MS (UCT)
Ing. Věra Schrenková Raman optical activity (ROA), Vibrational circular dichroism (VCD), theoretical calculations in spectroscopy (IOCB CAS)
Mgr. Kseniya Dryahina, Ph.D. Soft chemical ionization mass spectrometry (SIFT-MS, SESI-MS) and its applications to trace gas analysis (JH IPC CAS)
RNDr. Oldřich Benada, CSc. Electron microscopy and X-ray microanalysis and their applications in nanoparticles research (MBU CAS)
Assoc. Prof. Pavel Dvořák, Ph.D. Photoluminiscence (FS MU)

IAC CAS – Institute of Analytical Chemistry, Czech Academy of Sciences
IOCB CAS - Institute of Organic Chemistry and Biochemistry, Czech Academy of Sciences
FS CU – Faculty of Science, Charles University, Prague
FS MU – Faculty of Science, Masaryk University, Brno
UCT – University of Chemistry and Technology Prague
JH IPC CAS – J. Heyrovský Institute of Physical Chemistry, Czech Academy of Sciences
MBU CAS – Institute of Microbiology, Czech Academy of Sciences

Literature -

Last update: RNDr. Jan Kratzer, Ph.D. (10.02.2022)

Handbook of High-resolution Spectroscopy. Wiley 2011
Laser Chemistry. Spectroscopy, Dynamics, and Applications. Wiley 2007
Surface-Enhanced Raman Spectroscopy. Analytical, Bioanalytical, and Life Science Application. Wiley 2010
Modern Spectroscopy. 4th Ed. Wiley 2004

Requirements to the exam -

Last update: RNDr. Jan Kratzer, Ph.D. (14.02.2024)

This subject will be finished by an oral exam. The exam will cover all topics lectured during the session. Active participation in the lectures and excursions (maximum absence 20 %) is required.

Syllabus -

Last update: RNDr. Jan Kratzer, Ph.D. (10.02.2022)

Advanced spectrometric techniques used in atomic, molecular and mass spectrometry are discussed including their principles and applications. This year following techniques will be covered:

Raman spectroscopy, Raman optical activity (ROA), vibrational circular dichroism (VCD)

Single particle ICP-MS (sp-ICP-MS)

Speciation analysis by ICP-MS

Laser induced fluorescence (LIF) and two photon LIF (TALIF)

Optical emission spektrometry with high resolution in time and space

Electron microscopy (TEM, SEM)

X-ray microanalysis (EDS)

Ionization techniques for organic mass spectrometry (APCI, APPI, MALDI, ESI)

Ambient mass spectrometry