SubjectsSubjects(version: 953)
Course, academic year 2023/2024
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Inorganic Laboratory Course (a) - MC240C88
Title: Anorganické praktikum (a)
Czech title: Anorganické praktikum (a)
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2022
Semester: summer
E-Credits: 4
Examination process: summer s.:
Hours per week, examination: summer s.:0/8, C [DS]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: taught
Language: Czech
Explanation: Od 2022/23 garantem Dr. Martin Hulla (místo Doc. Kubíčka)
Additional information: http://dl2.cuni.cz/course/view.php?id=1794
Note: enabled for web enrollment
Guarantor: Martin Hulla, Ph.D.
Teacher(s): doc. RNDr. Róbert Gyepes, Dr., Ph.D.
Martin Hulla, Ph.D.
prof. RNDr. Jan Kotek, Ph.D.
doc. RNDr. Vojtěch Kubíček, Ph.D.
prof. Ing. Aleš Růžička, Ph.D.
Class: Sestava HPLC-MS
Incompatibility : MC240C10, MC240C11N, MC240C11NE, MC240C89
Pre-requisite : MC240P87
Is incompatible with: MC240C10, MC240C11N, MC240C13, MC240C12, MC240C89
Annotation -
Basic practical course dealing with synthesis and characterization of inorganic compounds. Students get training in syntheses of inorganic compounds by acid-base and oxidation-reduction reactions, complex formation reactions and reactions in melt.

Last update: Rubešová Jana, RNDr., Ph.D. (26.02.2018)
Literature -

Rohovec J.: (L)učebnice anorganické chemie, nakladatelství UK, Praha 2003
https://dl2.cuni.cz/course/view.php?id=1794

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (26.10.2019)
Requirements to the exam -

In the course, students are required to finish all preparations, to write reports and to pass a final exam.

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (28.08.2019)
Syllabus -
  1. Introduction.
    An overview of the common laboratory equipment. Ground glassware and its usage. Working with glass.
  2. Calculations in chemistry. Concentrations, chemical equations, preparation and mixing of solutions.
  3. Safety regulations in chemical laboratories. An overview of risks in labs. First aid after accident in laboratory.
  4. Acid-base reactions. Preparation of salts of common inorganic acids in aqueous solutions. Synthesis of salts of polybasic acids.
  5. Oxidation-reduction reactions. Preparation of elements and compounds containing ions in various oxidation states.
  6. Complex forming reactions. Synthesis of complex compounds of transition metal elements. Mono- and poly-dentate ligands. Common organic ligands in inorganic complexes.
  7. Preparation of elements and compounds at high temperature.
  8. Syntheses in non-aqueous solvents. Differences in the course of chemical reactions in non-aqueous solvents.

    In parts 4-8 students also get experience in isolation of inorganic compounds.
  9. Lab reports, publication of results.
Last update: Rubešová Jana, RNDr., Ph.D. (26.02.2018)
Entry requirements - Czech

Pro vstup do praktik je nezbytné získání zápočtu z předmětu Chemické výpočty a Laboratorní technika (a její varianty).
Další informace jsou k dispozici v aplikaci Moodle: https://dl2.cuni.cz/course/view.php?id=1794

Last update: Kubíček Vojtěch, doc. RNDr., Ph.D. (28.08.2019)
 
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