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Course, academic year 2023/2024
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Laboratory Exercises of Inorganic Chemistry - MC240C11M
Title: Anorganické praktikum (pro biochemiky)
Guaranteed by: Department of Inorganic Chemistry (31-240)
Faculty: Faculty of Science
Actual: from 2012
Semester: summer
E-Credits: 3
Examination process: summer s.:
Hours per week, examination: summer s.:0/5, C [DS]
Capacity: unlimited
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
State of the course: cancelled
Language: Czech
Is provided by: MC240C11N
Note: enabled for web enrollment
Guarantor: doc. RNDr. Vojtěch Kubíček, Ph.D.
Pre-requisite : MC250C01
Interchangeability : MC240C11N
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Annotation -
Last update: AGNEMEC (29.04.2005)
Basic practical course dealing with synthesis and characterization of inorganic compounds. Students get training in syntheses of inorganic compounds by acid-base and oxidation-reduction reactions, complex formation reactions and reactions in melt.

Literature - Czech
Last update: AGNEMEC (29.04.2005)

Literatura:

Podlaha J., Podlahová J.: Cvičení z preparativní anorganické chemie, nakladatelství UK, Praha 1993

Rohovec J.: (L)učebnice anorganické chemie, nakladatelství UK, Praha 2003

Syllabus -
Last update: AGNEMEC (29.04.2005)

1. Introduction

An overview of the common laboratory equipment. Ground glassware and its usage. Working with glass.

2. Calculations in chemistry. Concentrations, chemical equations, preparation and mixing of solutions.

3. Safety regulations in chemical laboratories. An overview of risks in labs. First aid after accident in laboratory.

4. Acid-base reactions. Preparation of salts of common inorganic acids in aqueous solutions. Synthesis of salts of polybasic acids. Iso- and hetero-polyacids and salts.

5. Oxidation-reduction reactions. Preparation of elements and compounds containing ions in unusually high or low oxidation states.

6. Complex forming reactions. Synthesis of complex compounds of transition metal elements. Mono- and poly-dentate ligands. Common organic ligands in inorganic complexes.

7. Preparation of elements and compounds at high temperature. Modern inorganic materials for material sciences and physical applications. Low melting alloys.

8. Syntheses in non-aqueous solvents. Preparation of materials in non-aqueous solvents. Differences in the course of chemical reactions in non-aqueous solvents.

In parts 4-8 students also get experience in isolation of inorganic compounds.

9. Lab reports, publication of results.

 
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