SubjectsSubjects(version: 901)
Course, academic year 2022/2023
  
Advances in Separation Science - MC230P63
Title: Advances in Separation Science
Guaranteed by: Department of Analytical Chemistry (31-230)
Faculty: Faculty of Science
Actual: from 2011
Semester: summer
E-Credits: 3
Examination process: summer s.:written
Hours per week, examination: summer s.:2/0 Ex [hours/week]
Capacity: unlimited
Min. number of students: unlimited
Virtual mobility / capacity: no
State of the course: taught
Language: English
Level: specialized
Note: enabled for web enrollment
priority enrollment if the course is part of the study plan
Guarantor: doc. RNDr. Tomáš Křížek, Ph.D.
Opinion survey results   Examination dates   Schedule   
Annotation
Last update: doc. RNDr. Tomáš Křížek, Ph.D. (11.05.2017)
The course deals with modern separation techniques such as UPLC, SFC, GCxGC and CZE. It will familiarize students with novelties in instrumentation, materials and application approaches.
The course is intended for students who already have basic knowledge of separation methods. The lecture is taught in English for Erasmus students but is open to all students.
The course is organized in so called "flipped class" format in which students are given materials prior to each class to read through them at home. In the class clarifications are provided if necessary and students apply the acquired knowledge to solve problems with teacher's assistance. Active participation of students in the learning process and student-oriented teaching yield better understanding and better fixation of the acquired knowledge.
Literature
Last update: doc. RNDr. Tomáš Křížek, Ph.D. (11.05.2017)

R. Smith (Series Editor): Handbook of Analytical Separation, Volume 1 - 6, Elsevier, Amsterdam.
R. Kellner: Analytical chemistry : A modern approach to analytical science (2nd edition), Wiley-VCH, Weinheim, 2004.
D. C. Harris: Quantitative Chemical Analysis (7th edition), W. H. Freeman, New York, 2007.

Study materials on each topic will be provided by teachers during the course. 

Requirements to the exam
Last update: doc. RNDr. Tomáš Křížek, Ph.D. (02.05.2019)

66% attendance is required. The course will be finished by a written exam covering all lectured topics. 

Syllabus
Last update: doc. RNDr. Tomáš Křížek, Ph.D. (19.01.2018)

HPLC - Modern stacionary phases. Introduction to UPLC.
CZE - Sample stacking methods. Enzyme assays. 
GCxGC
SFC
HPLC-MS

Examples of recent applications.

 
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