Subjects

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Special Methods of Instrumental Analysis - GF230

Title:	Speciální metody instrumentální analýzy
Form of teaching:	lecture+practicals
Guaranteed by:	Department of Analytical Chemistry (16-16140)
Faculty:	Faculty of Pharmacy in Hradec Králové
Actual:	from 2016
Duration in semesters:	1
Semester:	winter
Points:	0
E-Credits:	3
Examination process:	winter s.:oral
Hours per week, examination:	winter s.:1/3, C+Ex [HT]
Capacity:	unknown / unknown (56)
Maximum number of enrolled students:	56
Min. number of students:	unlimited
4EU+:	no
Virtual mobility / capacity:	no
Key competences:
State of the course:	not taught
Language:	Czech
Teaching methods:	full-time
Level:
Explanation:	(F 3.r.)
Repeated enrollment:	1 / 1 / - / 1
Note:	deregister from the exam date if a requisite was not fulfilled course can be enrolled in outside the study plan enabled for web enrollment

Guarantor:	doc. PharmDr. Hana Sklenářová, Ph.D. prof. RNDr. Dalibor Šatínský, Ph.D. doc. PharmDr. Petr Chocholouš, Ph.D.
Co-requisite :	GF274

Schedule

Annotation -

Theoretical fundamentals and practical training on selected instrumental analytical methods.

Last update: SOLICH/FAF.CUNI.CZ (21.08.2008)

Literature -

Rücker G., Neugebauer M.,Willems G.G.: Instrumentelle pharmazeutische Analytik, WVG Stuttgart 2001.

Robinson J.W., Skelly Frame E.M., Frame II G.M.. Undergraduate Instrumental Analysis, Marcel Dekker, New York, 2005

Klouda P.: Moderní analytické metody, nakladatelství Pavel Klouda, Ostrava 2003

Last update: SOLICH/FAF.CUNI.CZ (21.08.2008)

Teaching methods -

Lectures, seminars and practical training

Last update: SOLICH/FAF.CUNI.CZ (21.08.2008)

Course assessment methods and requirements for successful completion, grading scheme - Czech

Vypracování protokolů z absolvovaných úloh praktických cvičení.

Ústní zkouška podle požadavků uvedených v sylabech.

Last update: SOLICH/FAF.CUNI.CZ (23.06.2008)

Syllabus -

Introduction to special methods of instrumental analysis, classification of methods, principles.

Atomic-absorption spectrophotometry, absorbing medium, resonance spectral lines, instrumentation, analytical applications. Atomic-fluorescence spectrometry.

Luminescence analysis, fluorescence, phosphorescence, chemiluminescence, emission and excitation spectra, fluorimeters, spectrofluorimeters, qualitative and quantitative applications.

Turbidimetry and nephelometry

High-frequency spectroscopic methods, nuclear magnetic resonance, NMR spectrum, analytical applications, mass spectrometry, mass spectrum, analytical applications.

Electromigration methods, electrophoretic mobility, principles of separation. Capillary isotachophoresis , capillary zone electrophoresis, instrumentation, analytical applications.

Isoelectric focusation, micellar electrokinetic chromatography. Capillary electrochromatography. Instrumentation, applications.

Ion-exchange chromatography. Ion-exchange phenomena, cation and anion exchangers, ion-exchange equilibria, amino acid analyzers, molecular sieves, gel-permeation chromatography.

Pulse voltammetric methods. Difference pulse polarography. Stripping voltammetry.

Automation of analytical procedures, titrators, types of analyzers and their applications.

Flow-injection analysis, sequential injection analysis, automation of analytical procedures, principles, instrumentation, applications.

Last update: SOLICH/FAF.CUNI.CZ (21.08.2008)