Methods of Organic Structures Elucidation - GAF405
Title: Methods of Organic Structures Elucidation
Guaranteed by: Department of Organic And Bioorganic Chemistry (16-16120)
Faculty: Faculty of Pharmacy in Hradec Králové
Actual: from 2024
Semester: summer
Points: 0
E-Credits: 2
Examination process: summer s.:
Hours per week, examination: summer s.:0/28, C+Ex [HS]
Capacity: unknown / unlimited (10)
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
Key competences:  
State of the course: taught
Language: English
Teaching methods: full-time
Level:  
Note: deregister from the exam date if a requisite was not fulfilled
course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: doc. Dr. Russell Richard Anthony Kitson
Pre-requisite : GAF301
Interchangeability : GAF385
Examination dates   
Annotation
The subject is both theoretical (deepening of knowledge of spectral methods, especially NMR, then MS, IR and other methods used in many areas of chemical research), and practical (evaluation of NMR, IR, MS, ... data with an emphasis on identification of unknown compounds, correct interpretation and recording of characterization according to scientific standards). Students completing this subject will be prepared for the following scientific activity (diploma thesis, postgraduate studies, ...) and future career (pharmaceutical industry).
Last update: Matouš Petr, PharmDr., Ph.D. (15.02.2024)
Course completion requirements

The subject will not be opened in the academic year 2023/24

Last update: Matouš Petr, PharmDr., Ph.D. (15.02.2024)
Syllabus

Theoretical part:

  • properties of matter, separation, izolation of compounds
  • NMR, IR, MS, HR-MS, CHN analysis, polarimetry
  • X-ray crystallography
  • EMS, circular dichroism
  • identification of chiral compounds

Practical part:

  • interpretation of 1D NMR spectra
  • interpretation of IR and MS spectra
  • interpretation of other data (chiral compounds, dr, de, er, ee, etc.)
  • identification of unknown compounds
  • characterization of coumpounds
Last update: Matouš Petr, PharmDr., Ph.D. (15.02.2024)