SubjectsSubjects(version: 953)
Course, academic year 2023/2024
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Chemical Laboratory Technique - GAF369
Title: Chemical Laboratory Technique
Guaranteed by: Department of Organic And Bioorganic Chemistry (16-16120)
Faculty: Faculty of Pharmacy in Hradec Králové
Actual: from 2023
Semester: winter
Points: 0
E-Credits: 2
Examination process: winter s.:
Hours per week, examination: winter s.:0/56, C [HS]
Capacity: unknown / unlimited (unknown)
Min. number of students: unlimited
4EU+: no
Virtual mobility / capacity: no
Key competences:  
State of the course: taught
Language: English
Teaching methods: full-time
Teaching methods: full-time
Level:  
Note: deregister from the credit exam date if a requisite was not fulfilled
course can be enrolled in outside the study plan
enabled for web enrollment
Guarantor: doc. PharmDr. Mgr. Martin Krátký, Ph.D.
Comes under: 2.ročník 2023/24 Pharmacy (EN19)
Incompatibility : GAF130
Pre-requisite : GAF124, GAF285
Interchangeability : GAF130
Is co-requisite for: GAF035
Is interchangeable with: GAF130
Annotation -
The subject Chemical Laboratory Technique provides introduction to basic and advanced methods employed in a chemistry lab. Students will gain the knowledge about the function and equipment of a chemistry lab and will perform modern methods of synthesis, separation, purification and characterization of the resultant products.
Last update: Krátký Martin, doc. PharmDr. Mgr., Ph.D. (21.09.2023)
Course completion requirements -

Credit Requirements:  

•attendance at all practical classes

•completed protocols

•passing credit test (60 % of a total score is necessary)

•in the case of unfavorable epidemic situation wil be all details of accomplishment announced 

Last update: Krátký Martin, doc. PharmDr. Mgr., Ph.D. (21.09.2023)
Literature -

Obligatory:

  • Palát, Karel, Macháček, Miloš. Laboratory manual for general and inorganic chemistry : určeno pro posl. farmaceut. fakulty Univ. Karlovy. Praha: Karolinum, 1993, 109 s. ISBN 80-7066-751-6.

Last update: Krátký Martin, doc. PharmDr. Mgr., Ph.D. (21.09.2023)
Syllabus -

Syllabus:

  • Safety instructions
  • First aid in a chemistry lab
  • Introduction to chemistry lab
  • Laboratory glassware
  • Heating of the reaction mixtures - possible methods
  • Stirring of the reaction mixtures - possible methods
  • Methods of cooling of the reaction mixtures
  • Purification of solid chemicals - crystallization
  • Purification of liquid chemicals - distillation
  • Isolation of products
  • Extraction
  • Liquid and solid chemicals drying
  • Gases preparation and handling
  • Characterization of chemicals
  • Spectral methods in organic synthesis 
  • Thin-layer chromatography 
Last update: Krátký Martin, doc. PharmDr. Mgr., Ph.D. (21.09.2023)
Entry requirements -

Subject Chemical Laboratory Technique can be registered after passing subject General and Inorganic Chemistry (GAF124) and Organic Chemistry I (GAF285).

 

Last update: Krátký Martin, doc. PharmDr. Mgr., Ph.D. (21.09.2023)
 
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