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Last update: RNDr. Mgr. Tomáš Matoušek, Ph.D. (08.10.2020)
If the epidemiological measures would not allow teaching in person, the lectures will proceed in interactive online form, using appropriate technical means. |
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Last update: doc. RNDr. Karel Nesměrák, Ph.D. (28.10.2019)
Rita Cornelis, ed: Handbook of Elemental Speciation I, II; Wiley, 2005 |
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Last update: doc. RNDr. Karel Nesměrák, Ph.D. (28.10.2019)
Everything that was taught is tested. The exam is oral. |
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Last update: doc. RNDr. Karel Nesměrák, Ph.D. (28.10.2019)
1. What is speciation analysis: IUPAC definition, speciation and fractionation, specifics compared to trace element analysis, sources of information.
2. Methodology of speciation analysis - combination of separation and detection techniques (hyphenated techniques). 3. Methodology of speciation analysis - HPLC-ICPMS and ESI-MS 4. Speciation analysis methodology - speciation analysis methods based on volatile hydride generation. Excursion in laboratories UIACH AVČR (GC- and HPLC-ICP MS, hydride speciation techniques). 6. Collection, preservation and preparation of samples for speciation analysis. Quality assurance during derivatization and detection 7. Reference materials for speciation analysis, isotopic dilution, ICP-MS with laser ablation. Methods of analysis and specific application of individual elements: 8. Speciation analysis of arsenic 9. Speciation analysis of antimony, selenium and mercury 10. Special analysis of tin, lead, chromium, platinum 11. Problems of determination of nanoparticles. |